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[摘要]
应用毛细管气相色谱法,程序升温,FID检测器,同时测定食品中4种对羟基苯甲酸酯类防腐剂。该法线性范围为8l~800 g/ml,在此浓度范围内与峰面积呈良好的线性关系,方法的检出限为2.0~3.2 mg/kg,测定的回收率为78%~106%,相对标准偏差<11%。所建立的方法简便、快速、灵敏度高,并具有良好的精密度与准确度。
[Key word]
[Abstract]
Capillary gas chromatography was applied to the determination of 4 kinds of p-hydroxybenzoate antiseptics in foods. The recycle rate of this method and the detection limit were 78.2%~106.3% and 2.0 mg/kg~3.2 mg/kg, respectively. Besides, the linearity correlative coefficient exceeded 0.999.
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